NMR metabolomics as a complementary tool to brix-acid tests for navel orange quality control of long-term cold storage.

As expected for citrus fruit maturing on the tree, the stored fruit showed an increasing trend for Brix levels and a decreasing trend for percent Acids.

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The clustering of metabolites does not generate a notable trend in a collection of grouped metabolites.

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Given the juice metabolite data, there was a minor change in weekly citrate concentrations, with a slightly increasing trend.

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As expected for citrus fruit maturing on the tree, the stored fruit showed an increasing trend for Brix levels and a decreasing trend for percent Acids.

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Aspartate levels in the flavedo also had an interesting trend (Tables S1–S4 ).

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