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Time-resolved protein nanocrystallography using an X-ray free-electron laser.

Opt Express · 2012 · PMC3413412 · PMID 22330507

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an unexpected trendno p-value reported
While the decrease in signal at 10 μs was expected, the slight increase at 5 μs is an unexpected trend that has not been seen before in time resolved studies of reversible reactions by WAXS and Laue crystallography.

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Quoted from the open-access full text in Europe PMC under the licence the publisher applied. The sentence is reproduced exactly as published; the emphasis is ours.