HSQC NMR of the recovered lignins suggest a slight trend towards greater ether cleavage with increasing solids loading (Figure ESI-7 a).
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Process intensification of the ionoSolv pretreatment: effects of biomass loading, particle size and scale-up from 10 mL to 1 L.
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The sentences
It would lead to an apparent trend for increased ether cleavage without more pronounced condensation at higher loadings, while increasing pulp yield and decreasing lignin recovery.