Synthesis of piperidine and pyrrolidine derivatives by electroreductive cyclization of imine with terminal dihaloalkanes in a flow microreactor.

On the other hand, as shown in Table 4 , entries 3–5, the yield of 3a decreased slightly when the electricity was increased from 2.15 F mol −1 and above, and in contrast, there was an increasing trend in the yield of 4 .

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