For rGO‐SH (Figure 4b ) a clear trend emerges demonstrating an increase in scroll content with increasing pH (from 9.5% at pH 2.9 to 79.4% at pH 10.2 of 1D scroll structures), while reducing the amount of 2D flat structures (from 65% at pH 2.9 to 1.3% for pH 10.2 of 2D flat structures) with similar reduction for folded structures.
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