Chemometric Optimization of BF<sub>3</sub>·OEt<sub>2</sub>-Mediated Cyclization of Cannabidiol to Rare Δ⁴- and Iso-THC Isomers.

Although solvent alone was not significant, the solvent × BF 3 ·OEt 2 interaction approached significance, suggesting acetonitrile as the preferred medium to exploit this beneficial effect.

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Among linear and interaction terms, BF 3 ·OEt 2 equivalent exerts the greatest influence, while the quadratic effects are also highly significant.

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