While the majority of the cell volumes determined follow a clear trend, two of them were found to be outliners.
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The Biicosahedral Complex Anions [M(B<sub>11</sub>H<sub>11</sub>)<sub>2</sub>]<sup>3-</sup> (M = Cu, Ag, Au): Synthesis and Unexpected Low-Temperature Phase Transition of [Ag(η<sup>5</sup>-B<sub>11</sub>H<sub>11</sub>)<sub>2</sub>]<sup>3-</sup> to [Ag(η<sup>2</sup>-B<sub>11</sub>H<sub>11</sub>)<sub>2</sub>]<sup>3</sup>.
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