However, there is a clear trend between 675 and 710 °C of the peaks shifting to a higher 2θ, which indicates a contraction of the lattice.
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<i>In Situ</i> and <i>Ex Situ</i> X-ray Diffraction and Small-Angle X-ray Scattering Investigations of the Sol-Gel Synthesis of Fe<sub>3</sub>N and Fe<sub>3</sub>C.
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