Scalable Microreactor Concept for the Continuous Kolbe Electrolysis of Carboxylic Acids Using Aqueous Electrolyte.

[31] While further increasing the system pressure leaves the conversion constant at 39–40 %, the selectivity as well as the FE for Kolbe products show a decreasing trend.

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When different residence times were studied, the color of the aqueous phase after phase separation showed a trend from colorless over light yellow to a light orange color for higher residence times (see Supporting Information).

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