The linearity of the calibration curves was also proved by the values generated by the lack‐of‐fit F test (LOF), 19 always below the reported value of 3.58 ( α = 0.05; df1 = 6; df2 = 8), except for one of the seminal plasma curves, which showed a slightly significant lack of fit.
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Validation of a single liquid chromatography-tandem mass spectrometry approach for oxytetracycline determination in bull plasma, seminal plasma and urine.
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