MLA mappings ( Figure 4 ) highlighted a clear trend towards iron deficit/calcium excess, as the mass ratio progressed from 3:1 towards 1:3, with a mass ratio of 1:1 showing the highest levels of homogeneity (CFO-3, denoted as Ca 2 Fe 2 O 5 ).
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Optimisation of the Flame Spheroidisation Process for the Rapid Manufacture of Fe<sub>3</sub>O<sub>4</sub>-Based Porous and Dense Microspheres.
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In particular, and as highlighted in Table 3 , compositional differences were evident across the mass ratio sample set, with a strong trend towards the development of banded calcium iron oxide (CFO) compositions, the most prevalent of which being srebrodolskite (Ca 2 Fe 2 O 5 , denoted CFO-3—Ca 2 Fe 2 O 5 ; Supplementary Materials, Table S2 and Figure S1 ).