Ultrasonic-Assisted Silanization of SiO<sub>2</sub> Using TMSPM: Surface Functionalization, Hydrophobicity Enhancement, and Structural Analysis.

From Table , it can be concluded that there is a significant trend of concentration-dependent grafting of TMSPM molecules onto the surface of silica, as confirmed by a corresponding increase in the normalized intensity ratio of A (CO) / A ref (Si–O–Si) .

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The evolution of the microstructure in the thin film, as evidenced from the SEM images, indicates that there is a clear trend in the microstructure evolution that depends on the dopant concentration.

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